Journal: Marine Drugs

Article Title: Optimization and Validation of a High Throughput UHPLC-MS/MS Method for Determination of the EU Regulated Lipophilic Marine Toxins and Occurrence in Fresh and Processed Shellfish

doi: 10.3390/md20030173

Figure Lengend Snippet: Validation study.

Article Snippet: Standard stock solutions of LMTs in MeOH (OA, 8.37 mg L −1 ; DTX1; 8.52 mg L −1 ; DTX2, 3.78 mg L −1 ; PTX2, 4.41 mg L −1 ; AZA1, 1.30 mg L −1 ; AZA2, 1.22 mg L −1 ; AZA3, 1.18 mg L −1 ; YTX, 4.92 mg L −1 ; hYTX, 5.79 mg L −1 ) and freeze-dried mussel Certified Reference Material for Multiple Marine toxins (CRM-FDMT1, 3 g) were purchased from the National Research Council Canada NRCC (Halifax, Canada).

Techniques: Biomarker Discovery, Injection, Concentration Assay, Comparison, Standard Deviation

Journal: Marine Drugs

Article Title: Optimization and Validation of a High Throughput UHPLC-MS/MS Method for Determination of the EU Regulated Lipophilic Marine Toxins and Occurrence in Fresh and Processed Shellfish

doi: 10.3390/md20030173

Figure Lengend Snippet: Recent instrumental methods for the determination of lipophilic marine toxins.

Article Snippet: Standard stock solutions of LMTs in MeOH (OA, 8.37 mg L −1 ; DTX1; 8.52 mg L −1 ; DTX2, 3.78 mg L −1 ; PTX2, 4.41 mg L −1 ; AZA1, 1.30 mg L −1 ; AZA2, 1.22 mg L −1 ; AZA3, 1.18 mg L −1 ; YTX, 4.92 mg L −1 ; hYTX, 5.79 mg L −1 ) and freeze-dried mussel Certified Reference Material for Multiple Marine toxins (CRM-FDMT1, 3 g) were purchased from the National Research Council Canada NRCC (Halifax, Canada).

Techniques: Extraction, Biomarker Discovery